4.7 Article

Stereocontrolled synthesis of 20,21-dihydro N-methylwelwitindolinone B isothiocyanate

Journal

CHEMICAL COMMUNICATIONS
Volume 47, Issue 34, Pages 9705-9707

Publisher

ROYAL SOC CHEMISTRY
DOI: 10.1039/c1cc13498a

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Funding

  1. National Cancer Institute [NIH R01 CA101438]
  2. NATIONAL CANCER INSTITUTE [R01CA101438] Funding Source: NIH RePORTER

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Described is a concise synthesis of the 20,21-dihydro analog of N-methylwelwitindolinone B isothiocyanate, wherein a cationic homoallyl to cyclopropylmethyl rearrangement is circumvented by hydrogenation of the offending double bond.

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