Journal
CHEMICAL COMMUNICATIONS
Volume 47, Issue 39, Pages 11113-11115Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c1cc14599a
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Binuclear Fe-complexes that are readily prepared by treating Bu(4)N[Fe(CO)(3)(NO)] with an excess of thiol or from Fe-salts under reductive conditions are potent catalysts for the regioselective allylic sulfenylation. Low catalyst loadings of only 0.25 mol% and reaction temperatures of only 40 degrees C allow for the coupling of functionalized allylic starting materials with functionalized mercaptans in good yield with full retention of the configuration.
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