Journal
CHEMICAL COMMUNICATIONS
Volume 46, Issue 36, Pages 6852-6854Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c0cc01870h
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Funding
- National Natural Science Foundation of China [20902043, 20902042]
- Natural Science Foundation of Henan Province, China [102300410220]
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Hydroxylation of a monomeric triphenylphosphine-cyclopalladated ferrocenylchloropyrimidine [PdCl{[(eta(5)-C(5)H(5))]Fe[(eta(5)-C(5)H(3))-N(2)-C(4)H(2)-Cl]}(PPh(3))] with KOH gave the first example of a tetranuclear cluster monophosphine-palladacycle [Pd{[(eta(5)-C(5)H(5))]Fe[(eta(5)-C(5)H(3))-N(2)C(4)H(2)O]}(PPh(3))](4). Additionally, the analogous tricyclohexylphosphine tetranuclear cluster palladacycle has also been successfully synthesized by the same method.
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