Journal
CHEMICAL COMMUNICATIONS
Volume -, Issue 4, Pages 454-456Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/b817758a
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Funding
- NIBIB NIH HHS [R01 EB002807-30, R01 EB002807] Funding Source: Medline
- NATIONAL INSTITUTE OF BIOMEDICAL IMAGING AND BIOENGINEERING [R01EB002807] Funding Source: NIH RePORTER
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Between 65 and 175 K, nitroxyl radicals with spirocyclohexyl groups at the 2- and 6-positions of the piperidine ring exhibit spin echo dephasing rates that are slower than for nitroxyl radicals with 2,5-gem-dimethyl or 2,6-gem-dimethyl substituents that are currently used as spin labels, and are slow enough to permit DEER measurements at temperatures up to about 125 K for spin labels with analogous ring structures.
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