Journal
CHEMICAL & PHARMACEUTICAL BULLETIN
Volume 59, Issue 9, Pages 1169-1173Publisher
PHARMACEUTICAL SOC JAPAN
DOI: 10.1248/cpb.59.1169
Keywords
ring-closing metathesis; benzo[3,4]azepino[1,2-b]isoquinolinone; 3-arylisoquinoline; chemical shift difference
Funding
- Korea Research Foundation [KRF-2009-0071379]
- National Research Foundation of Korea [2009-0071379] Funding Source: Korea Institute of Science & Technology Information (KISTI), National Science & Technology Information Service (NTIS)
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Cycloaddition reaction between toluamides and benzonitriles was applied to prepare the 3-arylisoquinolines, and their chemical transformation to the dienes 4 was performed. The ring-closing metathesis (RCM) reaction afforded the desired heterocyclic compounds, benzo[3,4]azepino[1,2-b]isoquinolinones 5 in good yield.
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