Journal
CHEMICAL & PHARMACEUTICAL BULLETIN
Volume 57, Issue 11, Pages 1243-1245Publisher
PHARMACEUTICAL SOC JAPAN
DOI: 10.1248/cpb.57.1243
Keywords
diacetoxyiodobenzene; alpha,beta-unsaturated carboxylic acid; tetraethyl-ammonium bromide; bromoalkene
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A simple and mild method for the conversion of varieties of alpha,beta-unsaturated carboxylic acids to the corresponding bromoalkenes using diacetoxyiodobenzene (IBD) in combination with tetraethyl-ammonium bromide (TEAB) at room temperature is discussed. Advantages of this system are short reaction time, easy work up and gave good to excellent yields.
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