Journal
CHEMISTRY OF MATERIALS
Volume 12, Issue 1, Pages 22-+Publisher
AMER CHEMICAL SOC
DOI: 10.1021/cm990603d
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Ion exchange of Pd(II) ions into a nanostructured lyotropic liquid crystal network, followed by reduction with hydrogen gas, generates a polymer composite containing finely dispersed, catalytically active Pd nanoparticles 4-7 nm in diameter. Loss of order upon nanoparticle growth appears to be due to residual mobility in the polymer matrix near the ionic headgroups. The Pd nanoparticle composite exhibits excellent product selectivity in benzaldehyde hydrogenation and high reactivity in catalyzing Heck olefinations.
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