Journal
CHEMCATCHEM
Volume 5, Issue 1, Pages 277-283Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/cctc.201200496
Keywords
heterogeneous catalysis; nanomaterial; one-pot reaction; palladium; quinoline
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Funding
- Institute of Bioengineering and Nanotechnology (Biomedical Research Council, Agency for Science, Technology and Research, Singapore)
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The synthesis of quinolines has been achieved through a one-pot, two-step tandem reaction catalyzed with Ag-Pd alloy nanoparticles supported on carbon. Ag-Pd alloy nanoparticles catalyzed the coupling of a ketone with a primary alcohol through a hydrogen autotransfer process, which yields alpha-alkylated ketones under an Ar flow. These are reacted with 2-aminobenzyl alcohols in a modified Friedlander synthesis to give polysubstituted quinolines in moderate to good yields.
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