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JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 1
Volume -, Issue 22, Pages 2946-2957Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/b107180g
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The reaction of enolates of 1,3-dicarbonyl compounds with alpha -halo-alpha, beta -unsaturated carbonyl compounds affords 2,4-diacyldihydrofuran derivatives in the presence of DBU in THF. Chemical manganese dioxide oxidation of the hydrofurans leads to 2,4-diacylfuran derivatives. Application of the protocol enables short-step syntheses of antitumor naphthofuran natural products.
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