Journal
CERAMICS INTERNATIONAL
Volume 44, Issue 16, Pages 19686-19694Publisher
ELSEVIER SCI LTD
DOI: 10.1016/j.ceramint.2018.07.221
Keywords
Laminated ceramics; Thermal shock resistance; Indentation-quench method; Quenching-strengthening method
Categories
Funding
- Chinese National Foundation for Natural Sciences [51632007, 51672218]
- National Key R&D Program of China [2017YFB1103500]
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The thermal shock resistance (TSR) of laminated ZrB2-SiCw/BN ceramic was evaluated through indentation quench and quenching-strengthening methods. It was correspondingly compared to monolithic ZrB2-SiCw ceramic. In the indentation-quench method with consideration to crack propagation on the surface layer, the critical thermal shock temperature of laminated ZrB2-SiCw/BN ceramic with surface residual tensile stress was 550 degrees C, which was lower than monolithic ZrB2-SiCw/BN ceramic (600 degrees C). Unlike the microscopic method of crack growth measurement through indentation-quench testing, the quenching-strengthening method, which was based on the macroscopic properties of the material, mainly characterizing the residual strength subsequently to thermal shock, the critical thermal shock temperatures of the laminates and monolithic were 609 degrees C and 452 degrees C, respectively. Compared to the brittle fracture of ZrB2-SiCw ceramics, the deflection, bifurcation and delamination of the cracks as the main TSR mechanisms of the laminated ceramics, were revealed through quenching strengthening method, which was more suitable for the TSR characterization of laminated ceramics.
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