Journal
TETRAHEDRON LETTERS
Volume 43, Issue 1, Pages 119-121Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/S0040-4039(01)02096-2
Keywords
phosphorus compounds; anilides; elimination reaction; steric effects
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One of the o-t-butyl groups was eliminated from 2,4,6-tri-t-butyl-N-methylaniline by reaction with phosphorus trichloride in DME to afford sterically crowded N-(2,4-di-t-butylphenyl)-N-methylaminodichlorophosphine, which was utilized for preparation of a novel unsymmetrical diphosphene. (C) 2001 Elsevier Science Ltd. All rights reserved.
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