Journal
CHEMICAL COMMUNICATIONS
Volume -, Issue 12, Pages 1286-1287Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/b202846h
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Reaction of the lithium salt of 1,1-bis[2-(4,4-dimethyl) oxazolinyl]ethane (1) with 2-bromo-4,4-dimethyloxazoline yielded the novel tripodal ligand, 1,1,1- tris[2-(4,4-dimethyl) oxazolinyl]ethane (trisox-Me(2)2) which was reacted with one mol equivalent of [Cu(NCCH3)(4)](BF4) in dichloromethane to give [Cu(trisox-Me-2)](n)(BF4)(n) (3); while monomeric in solution, an X-ray diffraction study of 3 established a cyclic, centrosymmetric tetramer in the solid state.
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