Journal
CHEMISTRY OF MATERIALS
Volume 14, Issue 1, Pages 17-+Publisher
AMER CHEMICAL SOC
DOI: 10.1021/cm010820q
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We have developed a biphasic solvothermal synthesis for preparing hybrid inorganic-organic materials. The technique involves separation of metal and organic reactants using immiscible solvents. Crystallization takes place at the interface under solvothermal conditions. The technique has applications for promoting single-crystal growth, stabilizing easily reduced metal cations, and preparing phases that are unlikely to form under conventional hydrothermal conditions.
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