☆ 3.8 Article

Tungstophosphoric acid (H3PW12O40) as a heterogeneous inorganic catalyst. Activation of hexamethyldisilazane (HMDS) by tungstophosphoric acid for efficient and selective solvent-free O-silylation reactions

JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 1 (2002)

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Journal

JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 1
Volume -, Issue 23, Pages 2601-2604

Publisher

ROYAL SOC CHEMISTRY
DOI: 10.1039/b208202k

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Categories

Chemistry, Organic

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Tungstophosphoric acid (H3PW12O40) effectively activates hexamethyldisilazane for the selective silylation of primary, secondary, tertiary and phenolic hydroxy groups under solvent-free conditions at 55-60 degreesC.

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