Journal
TRANSITION METAL CHEMISTRY
Volume 27, Issue 2, Pages 196-199Publisher
KLUWER ACADEMIC PUBL
DOI: 10.1023/A:1013935602736
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Complexes of Cr-III, Mn-II, Fe-III, Co-II, Ni-II and Cu-II containing a macrocyclic pentadentate nitrogen-sulphur donor ligand have been prepared via reaction of a pentadentate ligand (N3S2) with transition metal ions. The N3S2 ligand was prepared by [1 +1] condensation of 2,6-diacetylpyridine with 1,2-di(o-aminophenylthio)ethane. The structures of the complexes have been elucidated by elemental analyses, molar conductance, magnetic susceptibility measurements, i.r., electronic and e.p.r. spectral studies. The complexes are of the high spin type and are six-coordinate.
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