Journal
JOURNAL OF CHEMICAL CRYSTALLOGRAPHY
Volume 33, Issue 11, Pages 845-849Publisher
KLUWER ACADEMIC/PLENUM PUBL
DOI: 10.1023/A:1027453612243
Keywords
nickel(II) complex; salicylaldehyde; o-phenylenediamine; crystal structure; Schiffbase
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A new complex has been synthesized and characterized by elemental analysis, IR, TGA, and single-crystal X-ray analysis. The crystal is orthorhombic and the space group is chiral (P2(1)2(1)2(1)) with a = 6.620(3) Angstrom, b = 17.300(4) Angstrom, c = 5.450(1) Angstrom, alpha = 90degrees, beta = 90degrees, gamma = 90degrees, z = 4. In the crystal lattice, the molecules create a two-dimensional network structure through hydrogen bonds. The C - H...O intermolecular hydrogen bonds connect the title complex to form a supermolecular structure.
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