Journal
NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH SECTION B-BEAM INTERACTIONS WITH MATERIALS AND ATOMS
Volume 199, Issue -, Pages 504-508Publisher
ELSEVIER SCIENCE BV
DOI: 10.1016/S0168-583X(02)01412-X
Keywords
iron phosphate; bismuth molybdate; hydrothermal; in situ; EDXRD; XRD/XAS; high surface area
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Iron phosphates and bismuth molybdate catalysts have been successfully prepared employing hydrothermal methods. In situ energy dispersive X-ray diffraction (EDXRD) and combined X-ray diffraction/X-ray absorption spectroscopy (XRD/XAS) studies reveal that these solid-state materials are formed from the amorphous precursor gel without the formation of any intermediate phases. While the time-resolved EDXRD measurements allowed us to determine the kinetics of phase formation, the combined XRD/XAS shows that there are local structural modifications taking place during the production of the crystalline active phases.: More importantly the materials prepared by this hydrothermal method possess a much higher surface area as compared to the ones prepared by conventional methods. (C) 2002 Elsevier Science B.V. All rights reserved.
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