Journal
SYNTHETIC COMMUNICATIONS
Volume 33, Issue 20, Pages 3631-3641Publisher
TAYLOR & FRANCIS INC
DOI: 10.1081/SCC-120024751
Keywords
melatonin; radical; synthesis; indole
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The hormone melatonin, which is known to have a range of important biological effects, has been prepared in a high-yielding route that features formation of the indole nucleus by radical cyclization. Mediation of the radical cyclization by tristrimethylsilylsilane (TTMSS) is more efficient than by N-ethylpiperidine hypophosphite.
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