Journal
JOURNAL OF MATERIALS CHEMISTRY
Volume 13, Issue 8, Pages 2007-2010Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/b305584a
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This paper presents the preparation of unique copper sulfide flakes in CTAB/n-C5H11OH/n-C6H14/ water microemulsions under hydrothermal conditions at 130 degreesC. With the pre-addition of n-dodecanethiol to the microemulsions, much smaller hexagonal Cu2S nanodisks resulted, which self-assembled into a superlattice. The crystal phases, absorption properties, and morphologies were characterized. The formation mechanism of the unique crystals is also discussed.
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