Journal
SYNTHETIC COMMUNICATIONS
Volume 33, Issue 1, Pages 119-126Publisher
TAYLOR & FRANCIS INC
DOI: 10.1081/SCC-120015567
Keywords
4H-benzo-[6]-pyran; arylmethylidenemalononitriles; 2-cyano-3-aryl-1-acrylate; synthesis
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A series of 5-oxo-5,6,7,8-tetrahydro-4H-benzo-[b]-pyran derivatives were prepared by the reaction of arylmethylidenemalononitriles or 2-cyano-3-aryl-1-acrylate with 5,5-dimethyl- 1, 3-cyclohexanedione (dimedone) in DMF at room temperature catalyzed by KF-alumina. The structure of the product was confirmed by X-ray analysis.
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