Journal
CARBON
Volume 41, Issue 14, Pages 2769-2777Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/S0008-6223(03)00388-9
Keywords
carbon black; catalyst support; small angle X-ray scattering
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Using a conventional laboratory diffractometer, small angle X-ray scattering (SAXS) was used to determine the average platinum particle size in samples of carbon with a range of platinum loadings. The results obtained were compared with those obtained from wide-angle X-ray diffraction (WAXS) studies. SAXS was more effective than WAXS for determining the average platinum particle size in samples where the grains were so small that the resultant diffraction peaks in the WAXS profiles were too broad to accurately determine the peak width for use in the Scherrer equation. (C) 2003 Elsevier Ltd. All rights reserved.
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