4.4 Article

The contribution of phonon scattering to high-resolution images measured by off-axis electron holography

Journal

ULTRAMICROSCOPY
Volume 98, Issue 2-4, Pages 115-133

Publisher

ELSEVIER SCIENCE BV
DOI: 10.1016/j.ultramic.2003.08.005

Keywords

phonon scattering; electron holography; high-resolution electron microscopy

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The contribution of electrons that have been phonon scattered to the lattice fringe amplitude and the background intensity of a high-resolution electron microscope (HREM) image is addressed experimentally through the analysis of a defocus series of energy-filtered off-axis electron holograms. It is shown that at a typical specimen thickness used for HREM imaging approximately 15% of the electrons that contribute to an energy-filtered image have been phonon scattered. At this specimen thickness, the phonon-scattered electrons contribute a lattice image of opposite contrast to the elastic lattice image. The overall lattice fringe contrast is then reduced to 70% of the value that it would have in the absence of phonon scattering. At higher specimen thickness, the behaviour is defocus-dependent, with the phonon image having lattice fringe contrast of either the same or the opposite sense to the elastic image as the defocus is varied. (C) 2003 Elsevier B.V. All rights reserved.

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