Journal
CATALYSIS TODAY
Volume 229, Issue -, Pages 95-103Publisher
ELSEVIER SCIENCE BV
DOI: 10.1016/j.cattod.2013.10.079
Keywords
Suzuki-Miyaura reaction; Plug flow reactor; XAS; Catalyst deactivation; Leaching
Funding
- Elucidate and Separate(ELSEP) - Palladium Catalysts in C-C and C-N Coupling Reactions [EP/G070172/1]
- Pharmacat Consortium (AstraZeneca, GlaxoSmithKline and Pfizer)
- Xunta Galicia
- Engineering and Physical Sciences Research Council [EP/G070172/1] Funding Source: researchfish
- EPSRC [EP/G070172/1] Funding Source: UKRI
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A custom-made plug flow reactor was designed and constructed to examine the behaviour of Pd catalysts during Suzuki-Miyaura cross-coupling reactions. Spatial-temporal resolution of catalyst activation, deactivation and leaching processes can be obtained by single-pass experiments. Subsequent deployment of the flow reactor in a XAS beam line revealed speciation of Pd along the catalyst bed. Crown Copyright (C) 2013 Published by Elsevier B.V. All rights reserved.
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