Journal
CATALYSIS LETTERS
Volume 142, Issue 11, Pages 1330-1335Publisher
SPRINGER
DOI: 10.1007/s10562-012-0911-4
Keywords
Synthesis; Decatungstate; Phase transfer; Selective oxidation; Self-separation; Recyclable
Categories
Funding
- National Natural Science Foundation of China [21103077]
- Program for New Century Excellent Talents in University (NCET) [NCET-11-1011]
- Liaoning Excellent Talents in University [LR201024, LJQ2011035]
- Natural Science Foundation of Liaoning Province [201102120, 201202123]
- Foundation of the Education Department of Liaoning Province [2010243, L2012128]
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A generalized synthesis method for decatungstate hybrids from bisulfate-based acidic ionic liquids was reported. N-butylpyridinium decatungstate [bPy](4)W10O32 and 1-butyl-3-methylimidazolium decatungstate [bmIm](4)W10O32 were synthesized and have been demonstrated to be good thermo-regulated phase transfer catalysts in an organic-solvent-free selective oxidation of alcohols under mild conditions. Advantages of heterogeneous and homogeneous catalysis are combined here, provided good self-separated and ease-of-recycling catalysts.
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