Journal
CATALYSIS COMMUNICATIONS
Volume 117, Issue -, Pages 57-62Publisher
ELSEVIER SCIENCE BV
DOI: 10.1016/j.catcom.2018.08.023
Keywords
Suzuki-Miyaura reaction; Aryl fluorosulfate; Potassium aryltrifluoroborate; One-pot; Terphenyls
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Funding
- NSFC [81660575, 81360471]
- Natural Science and Technology Foundation of Guizhou Province [[2018]1187]
- Scientific Research Foundation of Zunyi Medical University [E-234, F-807]
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A mild and efficient protocol has been developed for the Suzuki-Miyaura reaction of aryl fluorosulfates and potassium aryltrifluoroborates at room temperature. A series of biaryls can be prepared with excellent yields in this system and an aerobic atmosphere demonstrates a positive effect on the reactivity of the cross-coupling reactions. Additionally, this method can be extended to one-pot double Suzuki-Miyaura reactions, allowing the synthesis of various unsymmetrical terphenyls in moderate to good yields.
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