Journal
CATALYSIS COMMUNICATIONS
Volume 44, Issue -, Pages 24-28Publisher
ELSEVIER SCIENCE BV
DOI: 10.1016/j.catcom.2013.10.016
Keywords
Metal-organic framework; Cu-BDC; Hydrothermal synthesis; O-acetylation; Heterogeneous catalyst
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Funding
- Council of Scientific and Industrial Research (New Delhi, India)
- FCT/MCTES [CENIMAT/I3N, PEst-C/CTM/LA0025/2013-14, LA25-2013-2014]
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A novel metal-organic framework, Cu-BDC was synthesized by static hydrothermal method using innocuous solvents and characterized by several techniques such as powder XRD, ESR, TG-DTA, elemental analysis, ICP-AES, SEM, EDXS, FT-IR, BET surface area, pore volume and pore size. The catalytic performance of Cu-BDC was explored for O-acetylation of alcohols under solvent-free conditions at room temperature. The catalyst exhibited remarkable activity and reusability affording the desired products in excellent yields. (C) 2013 Elsevier B.V. All rights reserved.
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