Journal
CATALYSIS COMMUNICATIONS
Volume 17, Issue -, Pages 168-172Publisher
ELSEVIER SCIENCE BV
DOI: 10.1016/j.catcom.2011.10.015
Keywords
Fe3O4-NH2-Pd (0); Triethylene tetramine (TETA); Heterogeneous catalyst; Heck reaction
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Funding
- National Natural Science Foundation of China [50773063]
- National Basic Research Program of China [2010CB635111]
- Basic Research Foundation of Northwestern Polytechnical University [G9KY1020]
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A magnetically separable Fe3O4-NH2-Pd (0) catalyst was easily synthesized by immobilizing Pd nanoparticles on the surface of magnetic Fe3O4-NH2 microspheres. It was found that the combination of Fe3O4 and triethylene tetramine (TETA) could give rise to structurally stable catalytic sites. Furthermore, the high-magnetization Fe3O4-NH2-Pd(0) catalyst can be recovered by magnet and reused for six runs for Heck reaction without significant loss in catalytic activity. (C) 2011 Elsevier B.V. All rights reserved.
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