Journal
CATALYSIS COMMUNICATIONS
Volume 18, Issue -, Pages 5-10Publisher
ELSEVIER SCIENCE BV
DOI: 10.1016/j.catcom.2011.11.002
Keywords
TiO2-HCIO4; Silylation; Protect ion; Deprotection; Hexamethyldisilazane (HMDS)
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Funding
- University of Guilan Research Council
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TiO2-HCIO4, as a new solid acid, was found to be an efficient catalyst for the chemoselective trimethylsilylation of alcohols and phenols. Deprotection of the resulting trimethylsilylethers was achieved using the same catalyst in methanol solvent. The synthesized catalyst was characterized by FT-IR, SEM, TEM, BET and XRD analyses. Our novel synthetic method has the advantages of high yields, short reaction times, low cost and recyclability of the catalyst, simplicity and easy work-up compared to the conventional methods reported in the literature. (C) 2011 Elsevier B.V. All rights reserved.
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