Journal
CATALYSIS COMMUNICATIONS
Volume 9, Issue 6, Pages 1342-1345Publisher
ELSEVIER
DOI: 10.1016/j.catcom.2007.11.030
Keywords
cyanosilylation; aldehydes; N-iodosuccinimide; cyanohydrins
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An efficient protocol for the addition of TMSCN to aldehydes in CH2Cl2 by employing 0.5 mol%, of N-iodosuccinimide (NIS) as the catalyst is presented. A variety of aldehydes have been converted into the corresponding trimethylsilylethers within 15 min in excellent yield (up to 99%) under mild conditions. (C) 2007 Elsevier B.V. All rights reserved.
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