Journal
CHEMICAL COMMUNICATIONS
Volume -, Issue 21, Pages 2422-2423Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/b410293b
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Only two-fold amination occurs when 3 molar equivalents of TMPH are offered to a 1:1 BuNa-Bu2Mg mixture; adding TMEDA gives the mixed alkyl amide [(TMEDA)Na(mu-Bu)(mu-TMP) Mg(TMP)], which itself affords the phenyl-bridged analogue when reacted with benzene.
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