4.3 Article

The recovery of gas-vacancy-complexes in Fe irradiated with high energy H or He ions

Journal

MATERIALS TRANSACTIONS
Volume 45, Issue 1, Pages 9-12

Publisher

JAPAN INST METALS & MATERIALS
DOI: 10.2320/matertrans.45.9

Keywords

iron; hydrogen; helium; ion irradiation; positron annihilation spectroscopy; microvoids; gas-vacancy complex

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Isochronal annealing experiments for Fe irradiated with H or He ions were carried out to study interactions between gas atoms and vacancy clusters. The accelerating energy of H and He ions was 1.0 MeV and 3.3 MeV, respectively. The total dose was 1.0 x 10(21) H ions/m(2) (0.2dpa) and 9.6 x 10(19) He ions/m(2) (0.3 dpa), and the irradiation temperature was 300degreesC. Positron annihilation lifetime and coincidence Doppler broadening (CDB) measurements were carried out after irradiation and annealing for 1 hour up to the complete recovery temperature. Microvoids were detected after H or He ion irradiation. The characteristic difference was mainly shown in the recovery of vacancy type defects. The recovery of vacancy type defects introduced by H ion irradiation finished completely at 450degreesC, while that by He ion irradiation finished at 1000degreesC. It suggests that H-vacancy complexes were less stable than He-vacancy complexes. In addition, vacancy clusters formed by He ion irradiation grew after annealing at 600degreesC. This was caused by the emission of He atoms from small He-vacancy clusters and the coalescence between free vacancies and vacancy clusters, and by the migration and coalescence of He bubbles.

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