Journal
NEW JOURNAL OF CHEMISTRY
Volume 28, Issue 12, Pages 1499-1505Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/b410929e
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The crystal structures of the Cs+ salts of the halogenated monocarbaborane anions [closo-1-HCB9H4Br5](-), [closo-1-HCB11H5Cl6](-) and [closo-1-HCB11H5Br6](-) have been determined. The structures show two-dimensional extended-sheet or three-dimensional lattice structures and feature unusual distorted cuboctahedral and tetrakis hexahedral coordination geometries about Cs+. Incidental to the structural work, new convenient preparations of the precursive non-halogenated monocarbaborane anions [closo-1-HCB9H9](-) and [closo-1-HCB11H11](-) are presented.
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