Journal
HYPERFINE INTERACTIONS
Volume 165, Issue 1-4, Pages 101-106Publisher
SPRINGER
DOI: 10.1007/s10751-006-9252-2
Keywords
nanosized antimony particles; amorphous antimony; Sb-121 Mossbauer spectroscopy
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For the search of new negative electrodes of Li-ion batteries, a low-temperature method has been developed for the preparation of nanoscale antimony particles which uses an alkoxide-activated sodium hydride as reducing agent of antimony pentachloride. X-ray diffraction and TEM studies confirm the obtaining of amorphous Sb nanoparticles dispersed in an organic matrix. Sb-121 Mossbauer spectroscopy gives evidence for the occurrence of interactions between antimony and the matrix. These interactions are modified by the washing treatments.
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