Journal
OPTICAL MATERIALS
Volume 27, Issue 4, Pages 699-703Publisher
ELSEVIER SCIENCE BV
DOI: 10.1016/j.optmat.2004.09.012
Keywords
concentration distribution; TGT method; scanning electron microscopy; Leitz wide field microscopy; Laue photos
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Large ruby with the size of circle divide75 x 45 mm was grown by temperature gradient technique for the first time. Absorption spectrum was carried out in the range of 190-800 nm by spectrophotometer, and the concentration spatial distribution of Cr3+ in ruby was calculated from the absorption coefficient that based on the Beer-Lambert's Law. Cr3+ ions gradually increase alone both the growth axis and the radial direction. The shape and ingredient of the inclusions were measured by means of Leitz ride field microscopy and scanning electron microscopy. Lane photos and X-ray omega scan show the good quality of as grown ruby. The optimized growth conditions were pointed out based on the observation. (C) 2004 Elsevier B.V. All rights reserved.
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