Journal
CARBON
Volume 48, Issue 11, Pages 3205-3210Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.carbon.2010.05.005
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Graphite intercalation compounds (GICs) containing the tris(pentafluoroethyl)trifluorophosphate anion, [(C2F5)(3)PF3](-) are prepared for the first time by electrochemical oxidation of graphite in a nitromethane electrolyte. Powder X-ray diffraction (PXRD) data indicate that products are of stages 2-4 with gallery heights of 0.82-0.86 nm. Intercalate orientation is determined by using a structure model containing an energy minimized anion. GIC compositional parameters are obtained by microwave digestion followed by F elemental analysis, in combination with thermogravimetric analyses. (C) 2010 Elsevier Ltd. All rights reserved.
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