Journal
CARBOHYDRATE RESEARCH
Volume 393, Issue -, Pages 23-25Publisher
ELSEVIER SCI LTD
DOI: 10.1016/j.carres.2014.04.009
Keywords
Wittig reaction; exo-Glycals; Hydrogenation; Palladium catalyst; C-Glycosides
Funding
- Comision de Investigaciones Cientificas de la Provincia de Buenos Aires (CICPBA)
- UNLP
- CONICET
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Novel 2-deoxy-beta-benzyl-C-glycosides were prepared in good yields and excellent stereoselectivity by a route involving the Wittig reaction of glycosyl phosphonium salts and reduction of exo-glycals as key steps. Hydrogenation of benzyl protected enol ethers was performed with Pd/C(en) as an effective chemoselective catalyst to afford exclusively beta anomers. (C) 2014 Elsevier Ltd. All rights reserved.
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