Journal
CARBOHYDRATE RESEARCH
Volume 347, Issue 1, Pages 142-146Publisher
ELSEVIER SCI LTD
DOI: 10.1016/j.carres.2011.10.016
Keywords
Glycosylation; Trichloroacetimidate; Indium(III) promotion; InBr3; InCl3; In(OTf)(3)
Funding
- NIH [R01 GM62444]
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InCl3, InBr3, and In(OTf)(3) were tested as promoters in the preparation of glycosides from trichloroacetimidate precursors. A range of protecting groups and of alcohol acceptors were used to determine the versatility of these promoters. Disaccharide formation was demonstrated. In most cases, the In(III) compounds were shown to promote glycosylation better than the widely used promoter BF3 center dot OEt2. (C) 2011 Elsevier Ltd. All rights reserved.
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