Journal
CARBOHYDRATE RESEARCH
Volume 345, Issue 18, Pages 2714-2717Publisher
ELSEVIER SCI LTD
DOI: 10.1016/j.carres.2010.10.008
Keywords
Glycosylation; Carbohydrates; Natural products; Apigenin
Funding
- NNSF of China [20872172, 20732001, 20621703]
- National S&T Special Project [2009ZX09501-011]
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The first total synthesis of apigenin-4 -yl 2-O-(p-coumaroyl)-beta-D-glucopyranoside which exhibits good inhibitory activity against xanthine oxidase (XO) was accomplished in seven steps from a 1 2-blocked sugar unit and natural apigenin A unique allyl protecting group a phase-transfer-catalyzed (FTC) regioselective coupling reaction and robustness in large-scale preparation are the merits of this synthetic strategy (C) 2010 Elsevier Ltd All rights reserved
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