Journal
CARBOHYDRATE RESEARCH
Volume 345, Issue 6, Pages 740-749Publisher
ELSEVIER SCI LTD
DOI: 10.1016/j.carres.2010.01.011
Keywords
Glycosylation; Lewis acids; Solvent effects; Synthetic methods
Funding
- Ministry of Education, Culture, Sports, Science and Technology (MEXT), Japan [20790017]
- Kitasato University
- Grants-in-Aid for Scientific Research [20790017] Funding Source: KAKEN
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Efficient catalytic and stereoselective glycosylation was achieved by activating a glycosyl N-trichloroacetylcarbamate with a catalytic amount of Lewis acid in the presence of a glycosyl acceptor and 5 A molecular sieves. Catalytic one-pot dehydrative glycosylation of a 1-hydroxy carbohydrate was achieved stereoselectively by reaction with trichloroacetyl isocyanate, followed by activation with a catalytic amount of activators. (C) 2010 Elsevier Ltd. All rights reserved.
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