4.7 Article

Synthesis of methylcellulose-silver nanocomposite and investigation of mechanical and antimicrobial properties

Journal

CARBOHYDRATE POLYMERS
Volume 90, Issue 4, Pages 1818-1825

Publisher

ELSEVIER SCI LTD
DOI: 10.1016/j.carbpol.2012.07.082

Keywords

Silver nanoparticles; Methylcellulose; Composite materials; Films; Mechanical property; Antimicrobial activity

Funding

  1. UGC, Govt. of India
  2. DST under INSPIRE fellowship
  3. CSIR, New Delhi

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In this paper we reported preparation of methylcellulose-silver nanocomposite films by mixing of aqueous solution of methylcellulose with silver nitrate followed by casting. The silver nanoparticles were generated in methylcellulose matrix through reduction and stabilization by methylcellulose. The surface plasmon band at 412 nm indicated the formation of Ag nanoparticles. The MC-Ag nanocomposite films were characterized by X-ray diffraction (XRD), transmission electron microscopy (TEM) and Fourier transform infrared (FTIR). The X-ray diffraction analysis of synthesized MC-Ag nanocomposite films revealed that metallic silver was present in face centered cubic crystal structure. Average crystallite size of silver nanocrystal was 22.7 nm. The FTIR peaks of as-synthesized MC-Ag nanocomposite fully designated the strong interaction between Ag nanoparticles and MC matrix. Nano-sized silver modified methylcellulose showed enhanced mechanical properties i.e. the introduction of Ag leading to both strengthening and toughening of MC matrix. The methylcellulose-silver nanocomposite films offered excellent antimicrobial activity against various microorganisms. (C) 2012 Elsevier Ltd. All rights reserved.

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