4.7 Article

Effect of sucrose on dynamic mechanical characteristics of maize and potato starch films

Journal

CARBOHYDRATE POLYMERS
Volume 76, Issue 2, Pages 239-243

Publisher

ELSEVIER SCI LTD
DOI: 10.1016/j.carbpol.2008.10.016

Keywords

Starch film; Film tension; Sucrose; Dynamic mechanical characteristics; DMA

Funding

  1. National Natural Science Foundation of China [30800662]
  2. Science and Technology Support Project of China [2006BAD05A0401]
  3. Science and Technology Research Key Program of Chinese Ministry of Education [105014]
  4. Research and Development Fund for University's Doctoral Discipline of the Chinese Ministry of Education [20050019029]
  5. High Technology Research and Development Program of Chinese Ministry of Science and Technology [2006AA10256-02]

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The dynamic mechanical properties of prepared maize and potato starch films were evaluated for mixtures containing 0%, 10% and 15% (w/w) of sucrose at temperatures ranging from 40.0 to 140.0 degrees C. The spectra of storage modulus (G'), loss modulus (G ''), and loss factor (tan delta) of starch films were acquired. Remarkable reduction in the glass transition temperature of maize and potato starch films was observed with the increasing sucrose content. The spectra of storage modulus (G'), loss modulus (G ''), and loss factor (tan delta) were measured for the second and third time after two and seven days, respectively. The peaks of loss factor (tan delta) appeared at 59.81 +/- 1.86 degrees C and 95.96 +/- 1.67 degrees C after two-day-storage, but only one peak appeared at 85.46 +/- 5.50 degrees C after seven days. A shifting trend from higher to lower temperature for loss factor was observed after seven days. (C) 2008 Elsevier Ltd. All rights reserved.

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