Journal
ORGANIC & BIOMOLECULAR CHEMISTRY
Volume 3, Issue 10, Pages 1911-1921Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/b417941b
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The synthesis of aromatic dicarboxaldehydes is described along with their reactivity in the [3 + 3] cyclocondensation reaction with (1R, 2R)- diaminocyclohexane to give trianglimine macrocycles. In particular, the scope and limitation of the reaction with regard to complete control of the cavity size of the macrocycles is discussed producing a total of 11 macrocycles with different cavity sizes ranging from 9 to 23 &ANGS;.
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