Journal
SYNTHETIC COMMUNICATIONS
Volume 35, Issue 11, Pages 1501-1509Publisher
TAYLOR & FRANCIS INC
DOI: 10.1081/SCC-200057992
Keywords
green chemistry; microwave; phenol protection; silyl ethers
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A facile, time-saving procedure to protect phenols with tert-butyldimethylsilyl chloride using imidazole as catalyst under solvent-free conditions is described. Several phenolic compounds with different substitution patterns can be silylated in high yield with substantially reduced generation of residues, a present goal in organic synthesis.
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