Journal
SYNTHETIC COMMUNICATIONS
Volume 35, Issue 10, Pages 1351-1357Publisher
TAYLOR & FRANCIS INC
DOI: 10.1081/SCC-200057268
Keywords
2-amino-thiophene-3-carboxylic derivatives; microwave irradiation synthesis; solvent-free
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Under microwave irradiation and solvent-free conditions, cyanoacetates (cyanoacetamides) react with ketones and sulphur in the presence of a small amount of morpholine to give 2-amino-thiophene-3-carboxylic derivatives. In particular, tetrahydro-benzo[b]thiophene-3-carboxylic acid N-aryl amides were synthesized in high yields of 84-95%.
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