Journal
SYNTHETIC COMMUNICATIONS
Volume 35, Issue 1, Pages 79-87Publisher
TAYLOR & FRANCIS INC
DOI: 10.1081/SCC-200046503
Keywords
Alumina; Michel addition; microwave irradiation; solvent-free reactions; specific microwave effects
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Michael addition reaction between EMME and various O, S, N nucleophiles were investigated in the presence of catalysts such as KF, KOH, or K(OCCH3)(3) under solvent-free conditions either neat or on alumina as solid support. Compared to low reactivity of alcohols (40 to 80% yields according to aliphatic chain), aniline or thiophenol. gave good to excellent yields (90-99%).
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