Journal
HELVETICA CHIMICA ACTA
Volume 88, Issue 5, Pages 936-949Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/hlca.200590087
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Unexpectedly high retention times were obtained in HPLC investigations for compounds equipped with (C8F17CH2CH2)(3)Si tags on C8F17-modified silica gel (Fig. 4). Hence, these tags have a high potential for the noncovalent immobilization of catalysts to be applied in organic solvents, allowing for an easy separation and reuse of the catalyst by filtration and reapplication. The tris(perfluoroalkyl)silyl tag could be incorporated in a straightforward manner into ligands as demonstrated by the synthesis of several prominent classes of ligands (Schemes 4 - 6).
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