Journal
LETTERS IN ORGANIC CHEMISTRY
Volume 3, Issue 1, Pages 35-38Publisher
BENTHAM SCIENCE PUBL LTD
DOI: 10.2174/157017806774964521
Keywords
carbohydrates; regioselectivity; glycosides; acylation; glycosylations
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The regioselective 1-O-deacetylation of peracetylated carbohydrates with ammonium acetate in DMF (or a mixed solution of tetrahydrofuran and methanol) is described. It offers a facile and efficient way to prepare O-acetylpyranosides presenting one free hydroxyl group at the anomeric position.
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