Journal
JOURNAL OF NATURAL PRODUCTS
Volume 69, Issue 1, Pages 79-82Publisher
AMER CHEMICAL SOC
DOI: 10.1021/np0503449
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Four new Daphniphyllum alkaloids, daphnilongeranins A-D (1-4), along with four known ones, daphniphylline, longistylumphylline A, deoxyisocalyciphylline B, and daphnicyclidin D, were isolated from the leaves and stems of Daphniphyllum longeracemosum. Daphnilongeranin A (1) is the first seco-10, 17-longistylumphylline A type Daphniphyllum alkaloid, and daphnilongeranin B (2) is a new C-22 nor-Daphniphyllum alkaloid based on a new C-21 skeleton. Their structures and stereochemistry were determined using spectroscopic data and chemical methods.
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