Journal
ADVANCED SYNTHESIS & CATALYSIS
Volume 348, Issue 1-2, Pages 41-46Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/adsc.200505354
Keywords
asymmetric dihydroxylation; filtration-free; magnetic separation; mesoporous silca; recycling
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A new magnetic mesocellular mesoporous silica support featuring a 3D open-pore structure has been developed for highly efficient, filtration-free recycling of chiral ligands for catalytic asymmetric dihydroxylation. Reactions using the ligand immobilized on this magnetic silica system exhibited almost the same reactivity and enantioselectivity as those obtained in the homogeneous reaction. Magnetically recovered ligand could be recycled eight times with good to excellent conservation of reaction rates and enantioselectivities.
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