Journal
JOURNAL OF MAGNETIC RESONANCE
Volume 186, Issue 2, Pages 220-227Publisher
ACADEMIC PRESS INC ELSEVIER SCIENCE
DOI: 10.1016/j.jmr.2007.02.015
Keywords
solid-state NMR; quadrupolar nuclei; HETCOR; dipolar coupling; HMQC; R-INEPT
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We present several new methods that allow to obtain through-space 2D HETCOR spectra between spin-1/2 and half-integer quadrupolar nuclei in the solid state. These methods use the rotary-resonance concept to create hetero-nuclear coherences through the dipolar interaction instead of scalar coupling into the HMQC and refocused INEPT experiments for spin n/2 (n > 1). In opposite to those based on the cross-polarization transfer to quadrupolar nuclei, the methods are very robust and easy to set-up. (c) 2007 Elsevier Inc. All rights reserved.
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